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10,10-Dimethyl-l,2,8-thiadiazecan-9-one 1,1-dioxide


Linden, Anthony; Todorova, Tonya R; Heimgartner, Heinz (1999). 10,10-Dimethyl-l,2,8-thiadiazecan-9-one 1,1-dioxide. Acta Crystallographica. Section C: Crystal Structure Communications, 55:1378-1380.

Abstract

The puckered ten-membered ring of the title compound, C9HI8N2O3S, contains a sulfonamide group and an amide moiety which has the trans conformation. The molecules are linked into infinite two-dimensional networks by intermolecular N-H...O hydrogen bonds involving both NH groups along with the amide O atom and one of the sulfonyl O atoms from different neighbouring molecules. The title compound was prepared by a ring-enlargement reaction of the corresponding N-aminoalkyl 1,2-thiazetidin-3-one 1,1-dioxide.

Abstract

The puckered ten-membered ring of the title compound, C9HI8N2O3S, contains a sulfonamide group and an amide moiety which has the trans conformation. The molecules are linked into infinite two-dimensional networks by intermolecular N-H...O hydrogen bonds involving both NH groups along with the amide O atom and one of the sulfonyl O atoms from different neighbouring molecules. The title compound was prepared by a ring-enlargement reaction of the corresponding N-aminoalkyl 1,2-thiazetidin-3-one 1,1-dioxide.

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Additional indexing

Item Type:Journal Article, refereed, original work
Communities & Collections:07 Faculty of Science > Department of Chemistry
Dewey Decimal Classification:540 Chemistry
Language:English
Date:1999
Deposited On:05 Nov 2013 16:29
Last Modified:22 Nov 2017 13:40
Publisher:Wiley-Blackwell
ISSN:0108-2701
Funders:Swiss National Science Foundation, F. Hoffmann-La Roche AG, Basel
Publisher DOI:https://doi.org/10.1107/S0108270199007611

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