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Synthesis, characterization and applicability of three isotope labeled azobenzene photoswitches


Pfister, P; Ihalainen, J; Hamm, P; Kolano, C (2008). Synthesis, characterization and applicability of three isotope labeled azobenzene photoswitches. Organic & Biomolecular Chemistry, 6(19):3508-3517.

Abstract

We describe a short, efficient approach for the synthesis of three novel isotope labeled azobenzene photoswitches. Synthesis is based on commercially available fully isotope labeled precursors. The target molecules have been obtained in good yields, checked for purity, and identified by NMR and IR spectroscopy and a variety of standard analytical methods (UV/Vis, m.p., ESI-MS, elemental analysis). Using conventional coupling techniques the three isotope labeled photoswitches can be incorporated very easily in biomacromolecules.

Abstract

We describe a short, efficient approach for the synthesis of three novel isotope labeled azobenzene photoswitches. Synthesis is based on commercially available fully isotope labeled precursors. The target molecules have been obtained in good yields, checked for purity, and identified by NMR and IR spectroscopy and a variety of standard analytical methods (UV/Vis, m.p., ESI-MS, elemental analysis). Using conventional coupling techniques the three isotope labeled photoswitches can be incorporated very easily in biomacromolecules.

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Additional indexing

Item Type:Journal Article, refereed, original work
Communities & Collections:07 Faculty of Science > Department of Chemistry
Dewey Decimal Classification:540 Chemistry
Language:English
Date:7 October 2008
Deposited On:14 Jan 2009 15:00
Last Modified:06 Dec 2017 16:12
Publisher:Royal Society of Chemistry
ISSN:1477-0520
Publisher DOI:https://doi.org/10.1039/b804568b
PubMed ID:19082151

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