Publication: Crystal structure of tris(4,7-diphenyl-1,10-phenanthroline-κ2N,N′)cobalt(III) tris(hexafluorophosphate) monohydrate
Crystal structure of tris(4,7-diphenyl-1,10-phenanthroline-κ2N,N′)cobalt(III) tris(hexafluorophosphate) monohydrate
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Mani, A., Belgaied, J. E., Gasser, G., & Blacque, O. (2022). Crystal structure of tris(4,7-diphenyl-1,10-phenanthroline-κ2N,N′)cobalt(III) tris(hexafluorophosphate) monohydrate. Acta Crystallographica Section E: Crystallographic Communications, 78(3), 313–316. https://doi.org/10.1107/s2056989022001359
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The title compound, Co(C72H48N6)3·H2O, crystallizes with one tripositive complex molecule, three hexafluorophosphate anions and one solvent molecule of water in the asymmetric unit. The N6 coordination set around the central CoIII atom defines a distorted octahedral environment. Four fluorine atoms of one hexafluorophosphate anion are disordered over two sets of positions with site-occupancy factors of 0.697 (5) and 0.303 (5). In the crystal, intermolecular π–π stacking interactions, C—H...π, C—H...F and O—H...F and in
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- Mani, Asma
- Belgaied, Jamel Eddine
- Gasser, Gilles
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Mani, A., Belgaied, J. E., Gasser, G., & Blacque, O. (2022). Crystal structure of tris(4,7-diphenyl-1,10-phenanthroline-κ2N,N′)cobalt(III) tris(hexafluorophosphate) monohydrate. Acta Crystallographica Section E: Crystallographic Communications, 78(3), 313–316. https://doi.org/10.1107/s2056989022001359
