Publication: A multi-sample 94GHz dissolution dynamic-nuclear-polarization system
A multi-sample 94GHz dissolution dynamic-nuclear-polarization system
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Batel, M., Krajewski, M., Weiss, K., With, O., Däpp, A., Hunkeler, A., Gimersky, M., Pruessmann, K. P., Boesiger, P., Meier, B. H., Kozerke, S., & Ernst, M. (2012). A multi-sample 94GHz dissolution dynamic-nuclear-polarization system. Journal of Magnetic Resonance, 214(1), 166–174. https://doi.org/10.1016/j.jmr.2011.11.002
Abstract
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We describe the design and initial performance results of a multi-sample dissolution dynamic-nuclear-polarization (DNP) polarizer based on a Helium-temperature NMR cryostat for use in a wide-bore NMR magnet with a room-temperature bore. The system is designed to accommodate up to six samples in a revolver-style sample changer that allows changing samples at liquid-Helium temperature and at pressures ranging from ambient pressure down to 1mbar. The multi-sample setup is motivated by the desire to do repetitive in vivo measurements and
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Batel, M., Krajewski, M., Weiss, K., With, O., Däpp, A., Hunkeler, A., Gimersky, M., Pruessmann, K. P., Boesiger, P., Meier, B. H., Kozerke, S., & Ernst, M. (2012). A multi-sample 94GHz dissolution dynamic-nuclear-polarization system. Journal of Magnetic Resonance, 214(1), 166–174. https://doi.org/10.1016/j.jmr.2011.11.002