Publication: Synthesis, characterization and crystal structures of 2-[(E)-2-(4-hydroxy-3,5-dimethylphenyl)-1-diazenyl]benzoic acid and its polymeric and monomeric triorganotin(IV) complexes
Synthesis, characterization and crystal structures of 2-[(E)-2-(4-hydroxy-3,5-dimethylphenyl)-1-diazenyl]benzoic acid and its polymeric and monomeric triorganotin(IV) complexes
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Basu Baul, T. S., Paul, A., & Linden, A. (2012). Synthesis, characterization and crystal structures of 2-[(E)-2-(4-hydroxy-3,5-dimethylphenyl)-1-diazenyl]benzoic acid and its polymeric and monomeric triorganotin(IV) complexes. Journal of Organometallic Chemistry, 696(26), 4229–4235. https://doi.org/10.1016/j.jorganchem.2011.09.018
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Three triorganotin(IV) complexes of composition R3SnLH (R = Me, Bu and Ph and LH = 2-[(E)-2-(4-hydroxy-3,5-dimethylphenyl)-1-diazenyl]benzoate) have been synthesized and characterized by 1H-,13C-, 119Sn- NMR, and IR spectroscopic techniques in combination with elemental analysis. The crystal structures of the carboxylate ligand HO2CC6H4{N=N(C6H2-4-OH-3,5-(CH3)2)}-o in its neutral form and three triorganotin(IV) complexes, viz., polymeric (R3Sn[O2CC6H4{N-N(H)(C6H2-4-O-3,5-(CH3)2)}-o])n (R = Me (1) and Bu (2)) and monomeric Ph3Sn[O2CC6
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- Basu Baul, T S
- Paul, A
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Council of Scientific and Industrial Research, New Delhi, India (Grant No. 09/347/(0197)/2011/EMR I
Senior Research Fellowship, AP), the University Grants Commission, New Delhi, India through SAP-DSA, Phase III
Indo-Swiss Joint Research Programme, Joint Utilisation of Advanced Facilities (Grant No. JUAF 11, TSBB, AL)
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Basu Baul, T. S., Paul, A., & Linden, A. (2012). Synthesis, characterization and crystal structures of 2-[(E)-2-(4-hydroxy-3,5-dimethylphenyl)-1-diazenyl]benzoic acid and its polymeric and monomeric triorganotin(IV) complexes. Journal of Organometallic Chemistry, 696(26), 4229–4235. https://doi.org/10.1016/j.jorganchem.2011.09.018
