Publication: Total Synthesis and Structural Revision of Mangrolide D
Total Synthesis and Structural Revision of Mangrolide D
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Hattori, H., Hoff, L. V., & Gademann, K. (2019). Total Synthesis and Structural Revision of Mangrolide D. Organic Letters, 21, 3456–3459. https://doi.org/10.1021/acs.orglett.9b01256
Abstract
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Abstract
The unique 18-membered macrocyclic natural product mangrolide D was prepared in totally synthetic form. Key steps feature an Au-catalyzed glycosylation, aza-Michael addition, and LaLi3tris(binaphthoxide) catalyzed epoxidation. Detailed analysis of the constitution and configuration of the carbohydrate segment and the total synthesis of the revised structure led to structural revision of the originally proposed structure.
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- Hattori, Hiromu
- Hoff, Lukas V
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Hattori, H., Hoff, L. V., & Gademann, K. (2019). Total Synthesis and Structural Revision of Mangrolide D. Organic Letters, 21, 3456–3459. https://doi.org/10.1021/acs.orglett.9b01256
