Publication: A new crystal modification of diammonium hydrogen phosphate, (NH4)(2)(HPO4)
A new crystal modification of diammonium hydrogen phosphate, (NH4)(2)(HPO4)
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Kunz, P. C., Wetzel, C., & Spingler, B. (2010). A new crystal modification of diammonium hydrogen phosphate, (NH4)(2)(HPO4). Acta Crystallographica Section E: Crystallographic Communications, E66(Pt. 4), i26–i27. https://doi.org/10.1107/S1600536810009839
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The addition of hexafluoridophosphate salts (ammonium, silver, thallium or potassium) is usually used to precipitate complex cations from aqueous solutions. It has long been known that PF6- is sensitive towards hydrolysis under acidic conditions Gebala & Jones (1969). J. Inorg. Nucl. Chem. 31, 771-776; Plakhotnyk et al. (2005). J. Fluorine Chem. 126, 27-31]. During the course of our investigation into coinage metal complexes of diphosphine ligands, we used ammonium hexafluoridophosphate in order to crystallize Ag(diphosphine)(2)]PF6 c
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- Kunz, P C
- Wetzel, C
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Kunz, P. C., Wetzel, C., & Spingler, B. (2010). A new crystal modification of diammonium hydrogen phosphate, (NH4)(2)(HPO4). Acta Crystallographica Section E: Crystallographic Communications, E66(Pt. 4), i26–i27. https://doi.org/10.1107/S1600536810009839
