Publication: Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity
Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity
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Reith, L., Lienau, K., Cook, D. S., Moré, R., Walton, R. I., & Patzke, G. R. (2018). Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity. Chemistry, 24, 18424–18435. https://doi.org/10.1002/chem.201801565
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The hydrothermal growth of cobalt oxide spinel (Co3O4) nanocrystals from cobalt acetate precursors was monitored with in situ powder X‐ray diffraction (PXRD) in combination with ex situ electron microscopy and vibrational spectroscopy. Kinetic data from in situ PXRD monitoring were analyzed using Sharp–Hancock and Gualtieri approaches, which both clearly indicate a change of the growth mechanism for reaction temperatures above 185 °C. This mechanistic transition goes hand in hand with morphology changes that notably influence the phot
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- Reith, Lukas
- Lienau, Karla
- Cook, Daniel S
- Moré, René
- Walton, Richard I
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Reith, L., Lienau, K., Cook, D. S., Moré, R., Walton, R. I., & Patzke, G. R. (2018). Monitoring the Hydrothermal Growth of Cobalt Spinel Water Oxidation Catalysts: From Preparative History to Catalytic Activity. Chemistry, 24, 18424–18435. https://doi.org/10.1002/chem.201801565