Publication: Synthesis and reactions of a new cyclobutanethione derivative
Synthesis and reactions of a new cyclobutanethione derivative
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Mlostoń, G., Majchrzak, A., Rutkowska, M., Woznicka, M., Linden, A., & Heimgartner, H. (2005). Synthesis and reactions of a new cyclobutanethione derivative. Helvetica Chimica Acta, 88, 2624–2636. https://doi.org/10.1002/hlca.200590203
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The 3,3-dichloro-2,2,4,4-tetramethylcyclobutanethione (4b) was prepared from the parent diketone by successive reaction with PCl5 and Lawesson reagent in pyridine. This new thioketone 4b was transformed into 1-chlorocyclobutanesulfanyl chloride 5 and chloro 1-chlorocyclobutyl disulfide 9 by treatment with PCl5 and SCl2, respectively, in chlorinated solvents (Schemes 1 and 2). These products reacted with S- and P-nucleophiles by substitution of Cl− at the S-atom; e.g., the reaction with 4b yielded the di- and trisulfides 6b and 11, res
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- Mlostoń, Grzegorz
- Majchrzak, Agnieszka
- Rutkowska, Marzena
- Woznicka, Marta
- Heimgartner, Heinz
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Mlostoń, G., Majchrzak, A., Rutkowska, M., Woznicka, M., Linden, A., & Heimgartner, H. (2005). Synthesis and reactions of a new cyclobutanethione derivative. Helvetica Chimica Acta, 88, 2624–2636. https://doi.org/10.1002/hlca.200590203
