Publication: Synthesis of new Bis-imidazole derivatives
Synthesis of new Bis-imidazole derivatives
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Jasiński, M., Mlostoń, G., Mucha, P., Linden, A., & Heimgartner, H. (2007). Synthesis of new Bis-imidazole derivatives. Helvetica Chimica Acta, 90(9), 1765–1780. https://doi.org/10.1002/hlca.200790186
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The reaction of aldimines with alpha-(hydroxyimino) ketones of type 10 (1,2-diketone monooximes) was used to prepare 2-unsubstituted imidazole 3-oxides 11 bearing an alkanol chain at N(1) (Scheme 2, Table 1). These products were transformed into the corresponding 2H-imidazol-2-ones 13 and 2H-imidazole-2-thiones 14 by treatment with Ac2O and 2,2,4,4-tetramethylcyclobutane-1,3-dithione, respectively (Scheme 3). The three-component reaction of 10, formaldehyde, and an alkane-1,omega-diamine 15 gave the bis[1H-imidazole 3-oxides] 16 (Sche
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- Jasiński, M
- Mucha, P
- Heimgartner, H
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Jasiński, M., Mlostoń, G., Mucha, P., Linden, A., & Heimgartner, H. (2007). Synthesis of new Bis-imidazole derivatives. Helvetica Chimica Acta, 90(9), 1765–1780. https://doi.org/10.1002/hlca.200790186
