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Synthesis of Ferrocenyl and Ruthenocenyl Thioamide derivatives using a single-step three-component reaction

Patra, Malay; Hess, Jeannine; Konatschnig, Sandro; Spingler, Bernhard; Gasser, Gilles (2013). Synthesis of Ferrocenyl and Ruthenocenyl Thioamide derivatives using a single-step three-component reaction. Organometallics, 32(20):6098-6105.

Abstract

The efficient syntheses of various metallocenyl thioamides using a single-step three-component condensation reaction between the commercially available (dimethylaminomethyl)ferrocene or aminomethylferrocene and another organic amine in the presence of elemental sulfur are described. All new organometallic thioamide derivatives were unambiguously characterized by 1H and 13C NMR spectroscopy and mass spectrometry. Furthermore, the structures of five ferrocenyl thioamides determined by X-ray crystallography are presented.

Additional indexing

Item Type:Journal Article, refereed, original work
Communities & Collections:07 Faculty of Science > Department of Chemistry
Dewey Decimal Classification:540 Chemistry
Scopus Subject Areas:Physical Sciences > Physical and Theoretical Chemistry
Physical Sciences > Organic Chemistry
Physical Sciences > Inorganic Chemistry
Language:English
Date:2013
Deposited On:16 Dec 2013 11:45
Last Modified:09 Jun 2025 01:41
Publisher:American Chemical Society
ISSN:0276-7333
OA Status:Closed
Publisher DOI:https://doi.org/10.1021/om400715m
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