Publication: Multitopic 3,2′:6′,3′′-terpyridine ligands as 4-connecting nodes in two-dimensional 4,4-networks
Multitopic 3,2′:6′,3′′-terpyridine ligands as 4-connecting nodes in two-dimensional 4,4-networks
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Manfroni, G., Spingler, B., Prescimone, A., Constable, E. C., & Housecroft, C. E. (2022). Multitopic 3,2′:6′,3′′-terpyridine ligands as 4-connecting nodes in two-dimensional 4,4-networks. CrystEngComm, 24(40), 7073–7082. https://doi.org/10.1039/d2ce01130a
Abstract
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Abstract
The tetratopic 1,4-bis(2-phenylethoxy)-2,5-bis(3,2′:6′,3′′-terpyridin-4′-yl)benzene (1) and 1,4-bis(3-phenylpropoxy)-2,5-bis(3,2′:6′,3′′-terpyridin-4′-yl)benzene (2) ligands have been prepared and fully characterised. Combination of ligand 1 or 2 and [M(hfacac)2]·xH2O (M = Cu, x = 1; M = Zn, x = 2) under conditions of crystal growth by layering led to the formation of [Cu2(hfacac)4(1)]n·3.6n(1,2-Cl2C6H4)·2nCHCl3, [Zn2(hfacac)4(1)]n·nMeC6H5·1.8nCHCl3, [Cu2(hfacac)4(2)]n·nMeC6H5·2nH2O, [Cu2(hfacac)4(2)]n·2.8nC6H5Cl and [Cu2(hfacac)4(2)]
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Manfroni, G., Spingler, B., Prescimone, A., Constable, E. C., & Housecroft, C. E. (2022). Multitopic 3,2′:6′,3′′-terpyridine ligands as 4-connecting nodes in two-dimensional 4,4-networks. CrystEngComm, 24(40), 7073–7082. https://doi.org/10.1039/d2ce01130a
